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Abstract:

It is now almost 10 yr since radiocarbon dating of cremated bone was first developed using the small carbonate component contained within the hydroxyapatite-based inorganic fraction. Currently, a significant number of 14C laboratories date cremated bone as part of their routine dating service. As a general investigation of cremated bone dating since this initial development, a small, cremated bone intercomparison study took place in 2005, involving 6 laboratories. Six cremated bone samples (including 2 sets of duplicates), with ages spanning approximately 1500-2800 BP, were sent to the laboratories. The results, which showed relatively good agreement amongst the laboratories and between the duplicate samples, are discussed in detail. © 2007 by the Arizona Board of Regents on behalf of the University of Arizona.

Abstract:

Ultrafiltration of bone collagen provides a method of purification that can be very effective in reducing environmental contamination from soil-derived amino acids as well as removing degraded collagen or other short-chain proteins. The 91̽�� Radiocarbon Accelerator Unit (ORAU) first implemented ultrafiltration in the pretreatment of bone material for accelerator mass spectrometry (AMS) radiocarbon dating in 2000. However, the filters themselves contain carbonaceous material, and thus stringent quality control is required to demonstrate that this does not affect the accuracy of the dating. Here, we present quality assurance data from the bone pretreatment and dating program at ORAU, including dates on known-age and background-age bones over a range of sample sizes, and measurements of residual carbon contamination present in the filters after cleaning. © 2007 by the Arizona Board of Regents on behalf of the University of Arizona.

Abstract:

We present the first results of an accelerator mass spectrometry (AMS) radiocarbon intercomparison program on 3 different charcoal samples collected in one of the hearths of the Megaceros gallery of Chauvet Cave (Ardèche, France). This cave, rich in parietal decoration, is important for the study of the appearance and evolution of prehistoric art because certain drawings have been 14C dated to the Aurignacian period at the beginning of the Upper Paleolithic. The new dates indicate an age of about 32,000 BP, which is consistent with this attribution and in agreement with the results from the same sector of the cave measured previously at the Laboratoire des Sciences du Climat et de l'Environnement (LSCE). Six laboratories were involved in the intercomparison. Samples were measured in 4 AMS facilities: Center for Isotope Research, Groningen University, the Netherlands; the 91̽�� Radiocarbon Accelerator Unit, UK; the Centre de datation par le carbone 14, Univ. Claude Bernard Lyon 1, France (measured by AMS facilities of PoznaÒ University, Poland); and the LSCE, UMR CEACNRS-UVSQ, France (measured by the Leibniz-Labor of Christian-Albrechts-Universität Kiel, Germany). © 2007 by the Arizona Board of Regents on behalf of the University of Arizona.